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Information card for entry 8100881
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| Coordinates | Coordinates are not available: file is not found. |
|---|
| Formula | C33 H56 B F4 P2 Rh |
|---|---|
| Calculated formula | C33 H56 B F4 P2 Rh |
| SMILES | [Rh]1234([P](CC[P]1(C1CCCCC1)C1CCCCC1)(C1CCCCC1)C1CCCCC1)[CH]1=[CH]2C2[CH]3=[CH]4C1C2.[B](F)(F)(F)[F-] |
| Title of publication | Crystal structure of 1,2-bis(dicyclohexylphosphino)-ethane rhodium (I)-norborna-2,5-diene tetrafluoroborate, C~33~H~56~BF~4~P~2~Rh and of 1,2-bis(dicyclohexylphosphino)-ethane rhodium(I)-(Z,Z)-cycloocta- 1,5-diene tetrafluoroborate, C~34~H~60~BF~4~P~2~Rh · 1/2CH~3~OH |
| Authors of publication | Kempe, Rhett; Spannenberg, Anke; Drexler, Hans-Joachim; Heller, Detlef |
| Journal of publication | Zeitschrift für Kristallographie - New Crystal Structures |
| Year of publication | 2001 |
| Journal volume | 216 |
| Journal issue | 1 |
| Pages of publication | 165 - 168 |
| a | 18.829 ± 0.004 Å |
| b | 10.142 ± 0.002 Å |
| c | 17.411 ± 0.003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3324.9 ± 1.1 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 33 |
| Hermann-Mauguin space group symbol | P n a 21 |
| Hall space group symbol | P 2c -2n |
| Residual factor for significantly intense reflections | 0.033 |
| Weighted residual factors for significantly intense reflections | 0.0836 |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
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