#------------------------------------------------------------------------------ #$Date: 2024-08-03 08:56:24 +0100 (Sat, 03 Aug 2024) $ #$Revision: 293656 $ #$URL: svn://www.crystallography.net/cod/cif/9/00/84/9008416.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_9008416 loop_ _publ_author_name 'Koennecke M' 'Miehe G' 'Fuess H' _publ_section_title ;Static disorder of dodecasil 3C. A single-crystal study with synchrotron radiation Note: T = 523 K, split position refinement Locality: Synthetic ; _journal_name_full 'Zeitschrift fur Kristallographie' _journal_page_first 147 _journal_page_last 155 _journal_volume 201 _journal_year 1992 _chemical_formula_sum 'O2 Si' _chemical_name_common 'Dodecasil 3C' _space_group_IT_number 227 _symmetry_space_group_name_Hall '-F 4vw 2vw 3' _symmetry_space_group_name_H-M 'F d -3 m :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 19.369 _cell_length_b 19.369 _cell_length_c 19.369 _cell_formula_units_Z 136 _cell_volume 7266.438 _diffrn_ambient_temperature 523 _cod_original_sg_symbol_H-M 'F d 3 m' _cod_original_formula_sum 'Si17 O34.008' _cod_database_code 9008416 loop_ _symmetry_equiv_pos_as_xyz x,y,z x,1/2+y,1/2+z 1/2+x,y,1/2+z 1/2+x,1/2+y,z 3/4+z,1/2-x,1/4+y 3/4+z,-x,3/4+y 1/4+z,1/2-x,3/4+y 1/4+z,-x,1/4+y 3/4-y,1/2+z,1/4-x 3/4-y,+z,3/4-x 1/4-y,1/2+z,3/4-x 1/4-y,+z,1/4-x 3/4+x,1/2-y,1/4+z 3/4+x,-y,3/4+z 1/4+x,1/2-y,3/4+z 1/4+x,-y,1/4+z 3/4-z,1/2+x,1/4-y 3/4-z,+x,3/4-y 1/4-z,1/2+x,3/4-y 1/4-z,+x,1/4-y 3/4+y,1/2-z,1/4+x 3/4+y,-z,3/4+x 1/4+y,1/2-z,3/4+x 1/4+y,-z,1/4+x 3/4-x,1/2+y,1/4-z 3/4-x,+y,3/4-z 1/4-x,1/2+y,3/4-z 1/4-x,+y,1/4-z 1/2+x,3/4-z,1/4-y 1/2+x,1/4-z,3/4-y +x,3/4-z,3/4-y +x,1/4-z,1/4-y 1/2-z,3/4+y,1/4+x 1/2-z,1/4+y,3/4+x -z,3/4+y,3/4+x -z,1/4+y,1/4+x 1/2+y,3/4-x,1/4-z 1/2+y,1/4-x,3/4-z +y,3/4-x,3/4-z +y,1/4-x,1/4-z 1/2-x,3/4+z,1/4+y 1/2-x,1/4+z,3/4+y -x,3/4+z,3/4+y -x,1/4+z,1/4+y 1/2+z,3/4-y,1/4-x 1/2+z,1/4-y,3/4-x +z,3/4-y,3/4-x +z,1/4-y,1/4-x 1/2-y,3/4+x,1/4+z 1/2-y,1/4+x,3/4+z -y,3/4+x,3/4+z -y,1/4+x,1/4+z x,1/2+z,1/2+y x,+z,+y 1/2+x,1/2+z,+y 1/2+x,+z,1/2+y -z,1/2-y,1/2-x -z,-y,-x 1/2-z,1/2-y,-x 1/2-z,-y,1/2-x y,1/2+x,1/2+z y,+x,+z 1/2+y,1/2+x,+z 1/2+y,+x,1/2+z -x,1/2-z,1/2-y -x,-z,-y 1/2-x,1/2-z,-y 1/2-x,-z,1/2-y z,1/2+y,1/2+x z,+y,+x 1/2+z,1/2+y,+x 1/2+z,+y,1/2+x -y,1/2-x,1/2-z -y,-x,-z 1/2-y,1/2-x,-z 1/2-y,-x,1/2-z 3/4+z,1/4+x,1/2-y 3/4+z,3/4+x,-y 1/4+z,1/4+x,-y 1/4+z,3/4+x,1/2-y 3/4-y,1/4-z,1/2+x 3/4-y,3/4-z,+x 1/4-y,1/4-z,+x 1/4-y,3/4-z,1/2+x 3/4+x,1/4+y,1/2-z 3/4+x,3/4+y,-z 1/4+x,1/4+y,-z 1/4+x,3/4+y,1/2-z 3/4-z,1/4-x,1/2+y 3/4-z,3/4-x,+y 1/4-z,1/4-x,+y 1/4-z,3/4-x,1/2+y 3/4+y,1/4+z,1/2-x 3/4+y,3/4+z,-x 1/4+y,1/4+z,-x 1/4+y,3/4+z,1/2-x 3/4-x,1/4-y,1/2+z 3/4-x,3/4-y,+z 1/4-x,1/4-y,+z 1/4-x,3/4-y,1/2+z -z,3/4+x,3/4+y -z,1/4+x,1/4+y 1/2-z,3/4+x,1/4+y 1/2-z,1/4+x,3/4+y y,3/4-z,3/4-x y,1/4-z,1/4-x 1/2+y,3/4-z,1/4-x 1/2+y,1/4-z,3/4-x -x,3/4+y,3/4+z -x,1/4+y,1/4+z 1/2-x,3/4+y,1/4+z 1/2-x,1/4+y,3/4+z z,3/4-x,3/4-y z,1/4-x,1/4-y 1/2+z,3/4-x,1/4-y 1/2+z,1/4-x,3/4-y -y,3/4+z,3/4+x -y,1/4+z,1/4+x 1/2-y,3/4+z,1/4+x 1/2-y,1/4+z,3/4+x x,3/4-y,3/4-z x,1/4-y,1/4-z 1/2+x,3/4-y,1/4-z 1/2+x,1/4-y,3/4-z 1/4-x,1/2+z,3/4-y 1/4-x,+z,1/4-y 3/4-x,1/2+z,1/4-y 3/4-x,+z,3/4-y 1/4+z,1/2-y,3/4+x 1/4+z,-y,1/4+x 3/4+z,1/2-y,1/4+x 3/4+z,-y,3/4+x 1/4-y,1/2+x,3/4-z 1/4-y,+x,1/4-z 3/4-y,1/2+x,1/4-z 3/4-y,+x,3/4-z 1/4+x,1/2-z,3/4+y 1/4+x,-z,1/4+y 3/4+x,1/2-z,1/4+y 3/4+x,-z,3/4+y 1/4-z,1/2+y,3/4-x 1/4-z,+y,1/4-x 3/4-z,1/2+y,1/4-x 3/4-z,+y,3/4-x 1/4+y,1/2-x,3/4+z 1/4+y,-x,1/4+z 3/4+y,1/2-x,1/4+z 3/4+y,-x,3/4+z 3/4-x,3/4-z,y 3/4-x,1/4-z,1/2+y 1/4-x,3/4-z,1/2+y 1/4-x,1/4-z,y 3/4+z,3/4+y,-x 3/4+z,1/4+y,1/2-x 1/4+z,3/4+y,1/2-x 1/4+z,1/4+y,-x 3/4-y,3/4-x,z 3/4-y,1/4-x,1/2+z 1/4-y,3/4-x,1/2+z 1/4-y,1/4-x,z 3/4+x,3/4+z,-y 3/4+x,1/4+z,1/2-y 1/4+x,3/4+z,1/2-y 1/4+x,1/4+z,-y 3/4-z,3/4-y,x 3/4-z,1/4-y,1/2+x 1/4-z,3/4-y,1/2+x 1/4-z,1/4-y,x 3/4+y,3/4+x,-z 3/4+y,1/4+x,1/2-z 1/4+y,3/4+x,1/2-z 1/4+y,1/4+x,-z -z,-x,-y -z,1/2-x,1/2-y 1/2-z,-x,1/2-y 1/2-z,1/2-x,-y y,z,x y,1/2+z,1/2+x 1/2+y,z,1/2+x 1/2+y,1/2+z,x -x,-y,-z -x,1/2-y,1/2-z 1/2-x,-y,1/2-z 1/2-x,1/2-y,-z z,x,y z,1/2+x,1/2+y 1/2+z,x,1/2+y 1/2+z,1/2+x,y -y,-z,-x -y,1/2-z,1/2-x 1/2-y,-z,1/2-x 1/2-y,1/2-z,-x loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Si1 0.03130 0.03130 0.03220 0.00260 -0.00310 -0.00310 Si2 0.02760 0.02760 0.02760 -0.00040 -0.00040 -0.00040 Si3 0.02410 0.02410 0.02410 0.00000 0.00000 0.00000 O1 0.05500 0.11300 0.11300 -0.02500 -0.02500 -0.01800 O2 0.08200 0.08200 0.02900 -0.02900 0.01200 0.01200 O3 0.11600 0.10700 0.06300 -0.03900 0.00000 0.03300 O4 0.10500 0.10500 0.06100 -0.03200 0.00000 0.00000 O5 0.04300 0.04300 0.10700 -0.02300 0.00000 0.00000 O6 0.09500 0.05400 0.03200 -0.04700 -0.02600 0.01500 loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy Si1 0.06742 0.06742 0.37000 1.00000 Si2 0.21637 0.21637 0.21637 1.00000 Si3 0.12500 0.12500 0.12500 1.00000 O1 0.00000 0.34330 -0.34330 1.00000 O2 0.18870 0.18870 0.28890 0.50000 O3 0.20740 0.20590 0.29660 0.25000 O4 0.12500 0.12500 0.37910 0.50000 O5 0.12500 0.12500 0.36880 0.50000 O6 0.17280 0.18380 0.15490 0.16700 loop_ _cod_related_entry_id _cod_related_entry_database _cod_related_entry_code 1 AMCSD 0011022 2 AMCSD 0011024 loop_ _[local]_alternative_name_id _[local]_alternative_name_type _[local]_alternative_name_source _[local]_alternative_name_source_id _[local]_alternative_name_value 1 mineral AMCSD 0011022 "IMA2008-067" 2 mineral AMCSD 0011024 "Dodecasil 3C" _database_code_amcsd 0011022