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Information card for entry 4308866
Preview
| Coordinates | 4308866.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H52 Cl N2 O3 Os |
|---|---|
| Calculated formula | C36 H50 Cl N2 O3 Os |
| Title of publication | Chiral Osmium Complexes with Sterically Bulky Schiff-Base Ligands. Crystal Structures of Os(IV) Derivatives and the Reactivity and Catalytic Cyclopropanation of Alkenes with EDA |
| Authors of publication | Jing Zhang; Jiang-Lin Liang; Xian-Ru Sun; Hai-Bing Zhou; Nian-Yong Zhu; Zhong-Yuan Zhou; Philip Wai Hong Chan; Chi-Ming Che |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 3942 - 3954 |
| a | 18.688 ± 0.002 Å |
| b | 11.941 ± 0.001 Å |
| c | 20.078 ± 0.002 Å |
| α | 90° |
| β | 94.43 ± 0.02° |
| γ | 90° |
| Cell volume | 4467.1 ± 0.8 Å3 |
| Cell temperature | 301 ± 2 K |
| Ambient diffraction temperature | 301 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.1022 |
| Residual factor for significantly intense reflections | 0.0593 |
| Weighted residual factors for significantly intense reflections | 0.2019 |
| Weighted residual factors for all reflections included in the refinement | 0.2265 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.09 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
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