Crystallography Open Database

Information card for entry 4519411

4519410 << 4519411 >> 4519412

Preview

Coordinates	4519411.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H28 N2 O4 Si2
Calculated formula	C14 H28 N2 O4 Si2
SMILES	[Si]([Si](OC(=O)N1CCCC1)(C)C)(OC(=O)N1CCCC1)(C)C
Title of publication	Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior.
Authors of publication	Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin
Journal of publication	ACS omega
Year of publication	2022
Journal volume	7
Journal issue	11
Pages of publication	9527 - 9536
a	18.6575 ± 0.0005 Å
b	6.3147 ± 0.0001 Å
c	16.0768 ± 0.0004 Å
α	90°
β	96.139 ± 0.002°
γ	90°
Cell volume	1883.25 ± 0.08 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0475
Residual factor for significantly intense reflections	0.0374
Weighted residual factors for significantly intense reflections	0.0914
Weighted residual factors for all reflections included in the refinement	0.0963
Goodness-of-fit parameter for all reflections included in the refinement	1.103
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
274265 (current)	2022-04-03	cif/ Adding structures of 4519408, 4519409, 4519410, 4519411, 4519412, 4519413, 4519414 via cif-deposit CGI script.	4519411.cif