Crystallography Open Database

Information card for entry 4519412

4519411 << 4519412 >> 4519413

Preview

Coordinates	4519412.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H40 Cl6 N4 O8 Si2
Calculated formula	C23.999 H39.999 Cl5.997 N4 O8 Si2
Title of publication	Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior.
Authors of publication	Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin
Journal of publication	ACS omega
Year of publication	2022
Journal volume	7
Journal issue	11
Pages of publication	9527 - 9536
a	9.773 ± 0.0003 Å
b	11.6396 ± 0.0003 Å
c	16.0521 ± 0.0005 Å
α	86.509 ± 0.002°
β	75.909 ± 0.002°
γ	86.201 ± 0.002°
Cell volume	1765.26 ± 0.09 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0449
Residual factor for significantly intense reflections	0.0368
Weighted residual factors for significantly intense reflections	0.0909
Weighted residual factors for all reflections included in the refinement	0.0949
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
274265 (current)	2022-04-03	cif/ Adding structures of 4519408, 4519409, 4519410, 4519411, 4519412, 4519413, 4519414 via cif-deposit CGI script.	4519412.cif