Crystallography Open Database

Information card for entry 5000290

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Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H29 Cl4 Cu N3
Calculated formula	C16 H29 Cl4.009 Cu N3
Title of publication	Cu(I) and Cu(II) complexes of a pyridine-based pincer ligand
Authors of publication	Vedernikov, Andrei N.; Wu, Peng; Huffman, John C.; Caulton, Kenneth G.
Journal of publication	Inorganica Chimica Acta
Year of publication	2002
Journal volume	330
Journal issue	1
Pages of publication	103 - 110
a	10.7713 ± 0.0003 Å
b	16.2507 ± 0.0004 Å
c	13.1398 ± 0.0003 Å
α	90°
β	110.557°
γ	90°
Cell volume	2153.55 ± 0.1 Å³
Cell temperature	118 ± 2 K
Ambient diffraction temperature	118 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.0249
Weighted residual factors for all reflections included in the refinement	0.0221
Goodness-of-fit parameter for all reflections included in the refinement	0.5553
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

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