Crystallography Open Database

Information card for entry 5000291

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Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H50 Cl N P2 Ru
Calculated formula	C22 H50 Cl N P2 Ru
Title of publication	Geminal Dehydrogenation of Ether and Amine C(sp^3^)H~2~ Groups by Electron-Rich Ru(II) and Os
Authors of publication	Ferrando-Miguel, German; Coalter, III, Joseph N.; Gérard, Hélène; Huffman, John C.; Eisenstein, Odile; Caulton, Kenneth G.
Journal of publication	New Journal of Chemistry
Year of publication	2002
Journal volume	26
Journal issue	6
Pages of publication	687 - 700
a	21.4753 ± 0.0007 Å
b	8.8416 ± 0.0003 Å
c	13.4685 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	2557.35 ± 0.14 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for significantly intense reflections	0.0276
Weighted residual factors for all reflections included in the refinement	0.0307
Goodness-of-fit parameter for all reflections included in the refinement	0.8602
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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