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Information card for entry 7112102
Preview
| Coordinates | 7112102.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C93 H112 Cl4 Ge4 N8 |
|---|---|
| Calculated formula | C93 H112 Cl4 Ge4 N8 |
| Title of publication | Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond |
| Authors of publication | Yan Li; Kartik Chandra Mondal; Peter Stollberg; Hongping Zhu; Herbert W. Roesky; Regine Herbst-Irmer; Dietmar Stalke; Heike Fliegl |
| Journal of publication | Chem.Commun. |
| Year of publication | 2014 |
| Journal volume | 50 |
| Pages of publication | 3356 |
| a | 12.692 ± 0.002 Å |
| b | 12.839 ± 0.002 Å |
| c | 15.409 ± 0.003 Å |
| α | 98.61 ± 0.02° |
| β | 102.61 ± 0.02° |
| γ | 113.07 ± 0.03° |
| Cell volume | 2175.6 ± 0.9 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0323 |
| Residual factor for significantly intense reflections | 0.0258 |
| Weighted residual factors for significantly intense reflections | 0.0608 |
| Weighted residual factors for all reflections included in the refinement | 0.0639 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.051 |
| Diffraction radiation wavelength | 0.56086 Å |
| Diffraction radiation type | AgKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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Users of the data should acknowledge the original authors of the
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