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Information card for entry 7112103
Preview
| Coordinates | 7112103.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C18 H22 Ge N2 |
|---|---|
| Calculated formula | C18 H22 Ge N2 |
| Title of publication | Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond |
| Authors of publication | Yan Li; Kartik Chandra Mondal; Peter Stollberg; Hongping Zhu; Herbert W. Roesky; Regine Herbst-Irmer; Dietmar Stalke; Heike Fliegl |
| Journal of publication | Chem.Commun. |
| Year of publication | 2014 |
| Journal volume | 50 |
| Pages of publication | 3356 |
| a | 24.693 ± 0.003 Å |
| b | 10.903 ± 0.002 Å |
| c | 27.84 ± 0.003 Å |
| α | 90° |
| β | 114.96 ± 0.02° |
| γ | 90° |
| Cell volume | 6795 ± 2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0442 |
| Residual factor for significantly intense reflections | 0.0343 |
| Weighted residual factors for significantly intense reflections | 0.0772 |
| Weighted residual factors for all reflections included in the refinement | 0.0809 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
| Diffraction radiation wavelength | 0.56086 Å |
| Diffraction radiation type | AgKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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Users of the data should acknowledge the original authors of the
structural data.